As radio frequencies continued to increase during the early years of 'wireless' development, the use of quartz crystals as a stable reference source ran into a physical limitation because as crystal slices reached a certain thinness, overtone and subharmonics appeared that caused problems in circuits. A new mineral called tourmaline saved the day. With an elasticity much greater than quartz, tourmaline is able to vibrate at higher fundamental frequencies for a given thickness. Since that time, science has provided the means for utilizing the much more abundant quartz crystals in overtone modes so that tourmaline is not required. At the time, though, it was a much-welcomed alternative.
|April 1932 QST
of Contents]These articles are scanned and OCRed from old editions of the
ARRL's QST magazine. Here is a list of the
QST articles I have already posted. As time permits, I will
be glad to scan articles for you. All copyrights (if any) are hereby acknowledged.
Fundamental Crystal Control for Ultra-High Frequencies
Tourmaline Oscillators for Wavelengths Down to 1.2 Meters
By Harald Straubel
Fig. 1 - Lycopodium pattern of transverse oscillation of a quartz plate cut so that vibrations starting at the center are reflected simultaneously from the circumference. The powder thus collects at the central nodal point.
Fig. 2 - Lycopodium pattern on the surface of a "raw" tourmaline crystal plate that was cut perpendicular to the axis.
Fig. 3 - When the crystal of Fig. 2 was made circular the pattern of the oscillations became more symmetrical, as shown by the concentric rings of the lycopodium collected at the nodes.
Fig. 4 - Contrast this pattern of a disc-shaped quartz oscillator with those of the tourmaline shown in Fig. 3.
Fig. 5 - Ii the tourmaline crystal the optic and electric axis have the same direction.
Fig. 6 - The tourmaline controlled oscillator circuit. It is of the same type as the familiar circuit generally used for quartz crystal control.
Fig. 7 - Performance curve for an RE 134 valve with tourmaline crystals of the same diameter but of different thicknesses to give various wavelengths. The efficiency decreases rapidly at the shorter wavelengths.
Fig. 8 - An ultra-high frequency tourmaline crystal that was cracked near the edges from overloading without impairing its operation. The diameter of this plate is 8 millimeters (0.312 inch).
Fig. 9 - The tourmaline plate with respect to its three axes. The major surfaces are perpendicular to the optic (Z) axis and parallel to the plane of the X and Y axes.
Here is confirmation of exciting rumors that have been coming through from Germany since last fall. Practicable fundamental crystal control at the frequencies too high for quartz, has arrived. Tourmaline crystal does the trick. The pleasure of presenting this article is the keener because of the friendly cooperation of the A.R.R.L.'s sister societies, the D.A.S.D. and the R.S.G.B., that have brought it to us. The connection with the D.A.S.D. of Dr. Straubel, the author, and that with the R.S.G.B. of Mr. Pilpel, the translator, make this contribution a fine feather in the cap of amateur radio. - Editor.
The method of fundamental crystal control which has been used so far presents difficulties on frequencies higher than 6000 to 7500 kc. because very thin quartz oscillators produce side tones on several neighboring frequencies. This multiplicity of oscillations is noticeable even on longer waves but can be suppressed by cutting the quartz plate in a suitable shape. Fig. 1 shows such a plate. The surface and sides are ground so that all oscillations starting at the center will be reflected at the same time from the circumference of the crystal. The radius of the curves at the corners depends on the square root of the modulus of elasticity of quartz. If this plate is excited on its fundamental frequency, the whole plate oscillates in all directions. Lycopodium powder, uniformly distributed over the crystal plate, is therefore concentrated at the middle point, which is the nodal point of the whole disc.
For considerably higher frequencies than 6000-7500 kc. crystal-controlled short-wave transmitters nowadays do not often use this method, but employ quartz crystals with fundamental frequencies such as 3000 to 1500 kc., with frequency multiplication; that is to say, one uses harmonics of the crystal oscillator and amplifies them. An installation of this sort becomes very cumbersome and complicated when used on the ultra short waves because the harmonics are so weak that amplification must take place after every frequency doubling before further frequency doubling is practicable.
If it were possible to construct fundamental oscillators for such short waves, the installation would be extraordinarily simplified.
The tourmaline crystal controlled oscillator operates at 75 megacycles (4 meters) with the stability and other characteristics of quartz-crystal controlled oscillators operating at much lower frequencies. Imagine the number of frequency multiplying stages that would be necessary to duplicate its performance with quart-crystal control!
On the above-mentioned grounds, quartz is unsuitable for short-wave fundamental control. The author has found, however, that a tourmaline crystal produces considerably more uniform oscillations than quartz. It was noticed even with a "raw" crystal, a plate simply cut perpendicular to the optical axis, that on exciting the longitudinal oscillations, extraordinarily uniform transverse oscillations resulted, as shown in Fig. 2.
The piezo-electric constant of tourmaline is
i.e., about 10% less than quartz.
If, in spite of the smaller constants and the irregular natural formation of this crystal, particularly easy oscillations are noticeable, it is highly probable that this is because there is considerably less tendency to side-tone oscillation. Actually, in the natural crystal only a few symmetrical side tones could be detected and the frequencies of these were far removed from the fundamental.
From these results it can be assumed that the oscillating properties even of such a thin crystal will remain constant, as they must do if it is to be used for fundamental control of ultra short-wave transmitters. A further advantage for the production of very high frequencies lies in the high speed of sound, necessitated by the extraordinarily large elasticity modulus of 1,600,000 kilograms per square centimeter in the direction of the optical axis. Tourmaline, therefore, supplies a frequency 35% higher than quartz of the same thickness, the constant being 80 meters wavelength per millimeter thickness.1
Circuit and Tubes
A circuit for the production of the oscillations is shown in Fig. 6, while the photograph shows the actual transmitter for use on 7 meters and employing 5 watts. The simplicity of construction and absence of any type of screening are noticeable.
For waves down to 2 meters (150 mc.) ordinary detector or power valves were used (such as Telefunken RE 084 or RE 134), but for shorter waves a special short-wave valve was employed, the Valvo S 0401. For longer waves of 5 meters and upwards, a larger valve was found suitable, the RS 241, which is similar to the American Type '10 and the Philips TB 04/10. It was noticed that, as is usual with all self-excited transmitters, the higher the frequency the lower the efficiency, oscillation eventually ceasing altogether. Fig. 7 shows the performance of an RE 134 valve. The reason for this is partly the large self-capacity of the crystal which, for a given valve capacity, upsets the phase of the reaction on short waves to such an extent that the crystal no longer oscillates. The crystal then works only as short-circuit capacity while the valve either oscillates unstabilized or ceases to oscillate altogether. This can be avoided by reducing the capacity of the crystal, which can be done only by decreasing the diameter. An increase in the diameter does not enable the crystal to stand a greater load on these ultra short waves, however.
The electrodes next presented certain difficulties. Silvering,2 such as used in thick oscillators, must be omitted as this affects the fundamental frequency of the thin plate quite considerably and a great load will cause peeling, although the oscillator remains undamaged. Therefore, silvering was dispensed with and perfectly level electrodes were used. Even slight unevenness of the electrodes caused certain parts of the crystal to melt and become disintegrated. Splintering, such as occurs with quartz, was never experienced.
By using perfectly plane electrodes the load on the crystal could be considerably increased. Working temperatures of more than 100° Centigrade did not affect the operation in any way. Great overloading (crystal 8 mm. diameter, RS 241 Valve with 350 volts plate potential) once caused the edge of the crystal to crack without affecting the middle portion or causing the efficiency to decrease materially. (Fig. 8)
When the crystal was in a horizontal position, no extra weight was placed upon the electrodes. Although an additional weight reduced the crystal's controlling properties, it was possible, in the cases of crystals of larger diameter (12 mm.), to subject them to pressures up to 500 grams per square centimeter before they stopped oscillating. In order to render them safe from shocks and vibrations, a light spring was always used to supply pressure.
With the 75-mc. transmitter depicted experiments were carried out to determine the actual degree of frequency stabilization obtainable. The modulated transmissions were received on a simple detector with regeneration over a distance of 1 kilometer although no aerial was used for either transmitting or receiving. As far as the transmitter was concerned, no hand-capacity effects were noticed; but when the hand was placed near the inductance, reception was louder owing to the body acting as a capacity-coupled aerial. Only when the coil was actually touched did oscillation cease, to recommence immediately on the same frequency when the hand was removed. This was particularly noticeable when the transmitter was keyed in the plate circuit. The heterodyne note as heard in an oscillating receiver was absolutely pure on the frequency of 75 mc. (4 meters) and showed d no frequency change whatsoever, better than could be obtained when using a 7500-kc. quartz crystal. The well stabilized transmitted frequency in every case could be received on the detector with regeneration and without the need for the broad resonance curve of a super-regenerative receiver.
By varying the condenser C (Fig. 6) no jumping in frequency could be noticed. Naturally, the frequency of the tourmaline, just as that of quartz, was affected by varying the tuning of the plate circuit, but frequency jumping never took place. To obtain this condition, however, perfectly plane parallel crystal surfaces are necessary.
The temperature coefficient of tourmaline oscillators is about 10% greater than the average of quartz and is negative. Repeated measurements in the region of 20° to 60° Centigrade showed this coefficient to be 46.6 parts in a million per degree Centigrade. For an accurately constant frequency one must use a thermostat and heater, the cost of which is inconsiderable in comparison with the amount saved by the elimination of frequency-doubling and amplifying stages, and the simplification of the installation. For simple transmitters one can easily dispense with temperature control. The frequency change of tourmaline is always in proportion to the temperature variation.
Fig. 9 shows how the crystal plate is cut from the actual crystal. The position of the different axis is the same as in Fig. 5. Most suitable tourmaline crystals are found in Brazil and South Africa.3
In conclusion, I wish to offer my thanks to the firm of Carl Zeiss, Jena, Germany, for help in my experiments. In particular, without their great interest it would have been impossible to overcome the difficulties in construction of the shortest wave oscillators for 1.2 meters.
1. Converting to the English system and in terms of frequency, t=146.25f, approximately, where t is thickness in inches,
and f is frequency in kilocycles. The thickness dimension is parallel to the Z axis for tourmaline whereas it is generally
parallel to either the X or Y axis for quartz. - EDITOR.
2. Cf. Parsons, "Silvering Electrodes on Quartz Crystals," QST, March, 1932. - EDITOR.
3. We understand that the common black variety, known as schorl, is generally unsuitable. - EDITOR.
Posted April 18, 2013